TRI-O-TOLYLPHOSPHINE Chemical Properties | |
Melting point | 123-125 °C(lit.) |
storage temp. | Store below +30°C. |
form | Crystalline Powder |
color | White |
Water Solubility | Soluble in alcohol. Slightly soluble in cold water. Insoluble in water. |
Sensitive | air sensitive |
BRN | 661212 |
CAS DataBase Reference | 6163-58-2(CAS DataBase Reference) |
NIST Chemistry Reference | Phosphine, tris(2-methylphenyl)-(6163-58-2) |
EPA Substance Registry System | Phosphine, tris(2-methylphenyl)-(6163-58-2) |
Safety Information | |
Hazard Codes | Xi |
Risk Statements | 36/37/38 |
Safety Statements | 26-36-37/39 |
WGK Germany | 3 |
F | 10-23 |
TSCA | Yes |
TRI-O-TOLYLPHOSPHINE Usage And Synthesis | |
Chemical Properties | white to light yellow crystal powde |
Uses | suzuki reaction |
Purification Methods | It crystallises from EtOH [Boert et al. J Am Chem Soc 109 7781 1987]. [Beilstein 16 III 835.] |
TRI-O-TOLYLPHOSPHINE Preparation Products And Raw materials | |
Raw materials | Etanol-->Sodium hydroxide-->Hydrochloric acid-->Ethyl acetate-->Diethyl ether-->Tetrahydrofuran-->Dichloromethane-->PETROLEUM ETHER-->Sodium sulfate-->Sodium chloride-->Ammonium chloride -->Magnesium-->Phosphorus trichloride-->Iodine-->1,2-Dibromoethane-->L(+)-Tartaric acid-->2-Bromotoluene |
Preparation Products | 5-Methylindole |
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