N-(3-BROMOPROPYL)PHTHALIMIDE Chemical Properties | |
Melting point | 72-74 °C(lit.) |
Boiling point | 361℃ |
density | 1.578 |
refractive index | 1.6320 (estimate) |
Fp | 172℃ |
storage temp. | Store below +30°C. |
solubility | <1g/l |
form | Crystalline Powder or Crystals |
color | White to light beige |
BRN | 157547 |
InChIKey | VKJCJJYNVIYVQR-UHFFFAOYSA-N |
CAS DataBase Reference | 5460-29-7(CAS DataBase Reference) |
Safety Information | |
Risk Statements | 36/37/38 |
Safety Statements | 22-24/25 |
WGK Germany | 3 |
N-(3-BROMOPROPYL)PHTHALIMIDE Usage And Synthesis | |
Chemical Properties | white powder |
Purification Methods | Place it in a Soxhlet and extract it with Et2O, whereby the bis-phthalimido impurity is not extracted. Evaporate the Et2O and recrystallise the residue from EtOH, aqueous EtOH or pet ether. [Gabriel & Weiner Chem Ber 21 2669 1888, Gaudry Can J Chem 31 1060 1953, Beilstein 21/10 V 1277.] |
N-(3-BROMOPROPYL)PHTHALIMIDE Preparation Products And Raw materials | |
Preparation Products | N,N-DIBUTYL-1,3-PROPANEDIAMINE |
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