N-(9-Fluorenylmethoxycarbonyloxy)succinimide Chemical Properties | |
Melting point | 150-153 °C(lit.) |
Boiling point | 150-153°C |
density | 1.3460 (rough estimate) |
refractive index | 1.5000 (estimate) |
storage temp. | 2-8°C |
solubility | Soluble in dimethyl sulfoxide and dimethyl formamide. |
form | Microfine Powder |
color | White or almost white |
Sensitive | Moisture Sensitive |
BRN | 3569540 |
CAS DataBase Reference | 82911-69-1(CAS DataBase Reference) |
Safety Information | |
Hazard Codes | Xi,N,Xn |
Risk Statements | 36/37/38-51/53-43-22 |
Safety Statements | 22-24/25-26/37/39-26-61-37-24 |
RIDADR | UN 3077 9 / PGIII |
WGK Germany | 3 |
F | 10-21 |
Hazard Note | Moisture Sensitive |
HazardClass | 9 |
HS Code | 29251995 |
N-(9-Fluorenylmethoxycarbonyloxy)succinimide Usage And Synthesis | |
Chemical Properties | White powder |
Uses | Used in conjunction with Isothiocyanate to conduct partial Edman Degradation on biologically active peptides. |
Uses | N-protecting reagent for oligonucleotide and peptide syntheses |
Uses | Reagent for the preparation of pure Fmoc amino acids free from contamination by Fmoc-dipeptides. |
Purification Methods | Recrystallise the carbonate from CHCl3/Et2O, or from pet ether (b 40-60o). [Pauet Can J Chem 60 976 1982, Lapatsaris et al. Synthesis 671 1983.] |
N-(9-Fluorenylmethoxycarbonyloxy)succinimide Preparation Products And Raw materials | |
Preparation Products | [2-[2-(Fmoc-amino)ethoxy]ethoxy]acetic acid |
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