N,N,N',N'-Tetramethyl-p-phenylenediamine dihydrochloride Chemical Properties | |
Melting point | 222-224 °C(lit.) |
Boiling point | 378.54°C (rough estimate) |
density | 1.1961 (rough estimate) |
refractive index | 1.6400 (estimate) |
storage temp. | Store at RT. |
solubility | H2O: soluble500mg/10 mL |
form | powder |
color | off-white to gray |
Water Solubility | SOLUBLE |
Sensitive | Light Sensitive |
BRN | 5132096 |
Stability: | Stable. Incompatible with strong oxidizing agents, strong bases. |
CAS DataBase Reference | 637-01-4(CAS DataBase Reference) |
EPA Substance Registry System | 1,4-Benzenediamine, N,N,N',N'-tetramethyl-, dihydrochloride(637-01-4) |
Safety Information | |
Hazard Codes | Xi,Xn |
Risk Statements | 36/37/38-20/21/22-40 |
Safety Statements | 26-36-36/37-22-36/37/39 |
RIDADR | 2811 |
WGK Germany | 3 |
F | 8 |
TSCA | Yes |
HazardClass | 6.1(a) |
PackingGroup | II |
HS Code | 29215190 |
N,N,N',N'-Tetramethyl-p-phenylenediamine dihydrochloride Usage And Synthesis | |
Chemical Properties | Off white to gray powder |
Uses | An oxidizable compound |
Purification Methods | Crystallise the salt from isopropyl or n-butyl alcohols, saturated with HCl. Treat it with aqueous NaOH to give the free base (see previous entry) which is filtered, dried and sublimed in a vacuum. [Guarr et al. J Am Chem Soc 107 5104 1985, Beilstein 13 H 74.] |
N,N,N',N'-Tetramethyl-p-phenylenediamine dihydrochloride Preparation Products And Raw materials | |
Raw materials | Methanol-->Sulfuric acid -->Sodium chloride-->Acetone-->Calcium chloride-->Cuprous chloride-->Sodium bromide-->p-Phenylenediamine dihydrochloride |
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