| 4-Aminopyrimidine Chemical Properties | |
| Melting point | 154-156 °C(lit.) |
| Boiling point | 167.6°C (rough estimate) |
| density | 1.1031 (rough estimate) |
| refractive index | 1.5200 (estimate) |
| form | Crystals or Powder |
| pka | 5.71(at 20℃) |
| color | White to slightly beige |
| Water Solubility | Slightly soluble in water. |
| λmax | 273nm(EtOH)(lit.) |
| CAS DataBase Reference | 591-54-8(CAS DataBase Reference) |
| NIST Chemistry Reference | Pyrimidine, 4-amino-,(591-54-8) |
| Safety Information | |
| Hazard Codes | Xi |
| Risk Statements | 36/37/38 |
| Safety Statements | 26-37/39 |
| WGK Germany | 3 |
| 4-Aminopyrimidine Usage And Synthesis | |
| Chemical Properties | White to slightly beige crystals or powder |
| Purification Methods | Recrystallise 10.6g of aminopyrimidine from hot EtOAc (200mL) to give 7.4g colourless needles as first crop; evaporation to 25mL gives a second crop of 1.7g. The hydroiodide has m 180o. The picrate has m 225o. [Brown J Soc Chem Ind (London) 69 353 1950, Beilstein 24 H 81, 24 III/IV 2130.] |
| 4-Aminopyrimidine Preparation Products And Raw materials | |
| Preparation Products | 5-BROMOPYRIMIDIN-4-AMINE |
| Raw materials | Sodium hydroxide-->Hydrochloric acid-->Ethyl acetate-->Diethyl ether-->Sodium sulfate-->Ammonium hydroxide-->Ammonia-->Acetonitrile-->Formaldehyde-->Potassium permanganate-->CARBON DIOXIDE-->p-Anisidine-->Palladium hydroxide-->Potassium-->Sodium cyanoborohydride-->4-Amino-2,6-dichloropyrimidine-->Pyrimidine |
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