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  • Product Name:   1,1'-BIS(DI-TERT-BUTYLPHOSPHINO)FERROCENE
  • Synonyms:   1,1'-BIS(DI-T-BUTYLPHOSPHINO)FERROCENE;BIS[(DI-TERT-BUTYLPHOSPHINO)CYCLOPENTADIENYL]IRON;1,1'-Bis(di-t-butylphosphino)ferrocene,min.98%;1,1'-Bis(di-t-butylphosphino)ferrocene, min. 98%;98% DtBPF
  • CAS No.:   84680-95-5
  • Molecular Formula:   C26H44FeP2 10*
  • Molecular Weight :   474.42
  • Specification :   98%
  • Place of Origin:   China
  • Appearance :   
  • Document :   Download

Description of 1,1'-BIS(DI-TERT-BUTYLPHOSPHINO)FERROCENE
1,1'-BIS(DI-TERT-BUTYLPHOSPHINO)FERROCENE Chemical Properties
Melting point  181-182°C (dec.)
form  crystal
color  orange to red
Water Solubility  Insoluble in water.
InChIKey FPLSJBJGQLJLSV-UHFFFAOYSA-N
Safety Information
Hazard Codes  Xi
Risk Statements  36/37/38
Safety Statements  22-24/25-36/37/39-26
1,1'-BIS(DI-TERT-BUTYLPHOSPHINO)FERROCENE Usage And Synthesis
Reaction
  1. Ligand for synthesis of polycyclic indoles via Pd-catalyzed intramolecular heteroannulation.
  2. Ligand for the palladium-catalyzed intramolecular arylation of aryl bromides under mild conditions.
  3. Ligand for cross-coupling reactions between bromoarenes and potassium allyltrifluoroborates promoted by a catalyst prepared from Pd(OAc)2 and DTBPF selectively providing γ-coupling products.
  4. Ligand for the copper-catalyzed system for the ß-boration of of a variety of α,ß-unsaturated amides.
  5. Ligand for the synthesis of Paucifloral F and related indanone analogues via palladium-catalyzed α-arylation.
  6. Ligand for the Pd-carbon monoxide complex catalyzed hydroxycarbonylation of aryl halides.
  7. Ligand for the palladium-catalyzed β-C-glycosylation by decarboxylative allylation to normal pyran systems,and cis-2,6-disubstituted tetrahydropyrans.
  8. Pd-catalyzed dearomative indole bisfunctionalization via a diastereoselective arylcyanation.
  9. Ligand for the copper- DTBPF catalyzed C–H activation and carboxylation of terminal alkynes.
1,1'-BIS(DI-TERT-BUTYLPHOSPHINO)FERROCENE Preparation Products And Raw materials
Raw materials Ethyl acetate-->Tetrahydrofuran-->Dichloromethane-->n-Butyllithium-->Hexane-->Magnesium-->Phosphorus trichloride-->N,N,N',N'-Tetramethylethylenediamine-->2-Chloro-2-methylpropane-->Ferrocene-->Cinchonidine-->Di-tert-butylchlorophosphane-->sec-Butanol-->Cyclohexyl bromide-->2,2'-Dipyridyl

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