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  • Product Name:   Pyridinium chlorochromate
  • Synonyms:   PCC;chromate(1-),chlorotrioxo-,(beta-4)-,hydrogen,compd.withpyridine(1:1);Pyridine, (T-4)-chlorotrioxochromate(1-);Pyridine, chlorotrioxochromate(1-);Urine Luck
  • CAS No.:   26299-14-9
  • Molecular Formula:   C5H6ClCrNO3
  • Molecular Weight :   215.56
  • Specification :   98%
  • Place of Origin:   China
  • Appearance :   
  • Document :   Download

Description of Pyridinium chlorochromate
Pyridinium chlorochromate Chemical Properties
Melting point  205-208 °C(lit.)
storage temp.  2-8°C
solubility  Soluble in acetone, benzene, dichloromethane, acetonitrile and tetrahydrofuran.
form  Crystalline Powder
color  Orange
Sensitive  Moisture Sensitive
Merck  14,7974
Stability: Stable. May react with easily oxidized materials. Incompatible with reducing agents, combustible material, metals, strong reducing agents.
CAS DataBase Reference 26299-14-9(CAS DataBase Reference)
EPA Substance Registry System Chromate(1-), chlorotrioxo-, (T-4)-, hydrogen, compd. with pyridine (1:1)(26299-14-9)
Safety Information
Hazard Codes  O,T,N
Risk Statements  49-8-43-50/53-20/21/22
Safety Statements  53-45-60-61-37-24-17-44-36/37/39-22
RIDADR  UN 1479 5.1/PG 2
WGK Germany  2
TSCA  Yes
HazardClass  5.1
PackingGroup  III
HS Code  29333990
Pyridinium chlorochromate Usage And Synthesis
Chemical Properties orange crystalline powder
Uses Usually used to oxidize an allylic methylene group.
Uses Oxidizing agent in organic synthesis.
Purification Methods Dry it in a vacuum for 1hour. It is not hygroscopic and can be stored for extended periods at room temperature without change. If the purity is very suspect, it can be readily prepared. [Corey & Scuggs Tetrahedron Lett 2647 1975, Piancatelli et al. Synthesis 245 1982.] (Possible CARCINOGEN.) § Available commercially on a polymer support.
Pyridinium chlorochromate Preparation Products And Raw materials
Preparation Products 3-(TRIFLUOROMETHYL)-1-PHENYL-1H-PYRAZOLE-4-CARBALDEHYDE-->1,3-DIMETHYL-1H-PYRAZOLE-5-CARBALDEHYDE-->Tetrahydropyran-4-carbaldehyde-->3-(TRIFLUOROMETHYL)-1-METHYL-1H-PYRAZOLE-4-CARBALDEHYDE-->1-TERT-BUTYL-3-(TRIFLUOROMETHYL)-1H-PYRAZOLE-4-CARBALDEHYDE-->Cyclopropanecarboxaldehyde-->3-(2-METHOXY-PHENYL)-PROPIONALDEHYDE-->1-(2,6-DIFLUOROPYRIDIN-3-YL)PROPAN-1-ONE-->2-(4-Methylpiperazin-1-yl)-6-(trifluoromethyl)pyrimidine-4-carbaldehyde-->5-CHLORO INDAZOLE-3-CARBOXALDEHYDE-->3-(4-NITRO-PHENYL)-PROPIONALDEHYDE-->4-(MORPHOLIN-4-YLMETHYL)-1,3-THIAZOL-2-AMINE-->1-tert-Butoxycarbonyl-4-piperidinecarboxaldehyde-->3-(2,6-DICHLOROPHENYL)-5-METHYLISOXAZOLE-4-CARBALDEHYDE-->2,5-DIBROMONICOTINALDEHYDE-->TERT-BUTYL 4-(4-FORMYL-1,3-THIAZOL-2-YL)TETRAHYDRO-1(2H)-PYRIDINECARBOXYLATE-->TERT-BUTYL 4-(5-FORMYL-4-METHYL-1,3-THIAZOL-2-YL)PIPERIDINE-1-CARBOXYLATE-->5-BROMO-3-FORMYLPYRIDINE-->2-PHENYL-1,3-THIAZOLE-4-CARBALDEHYDE-->TERT-BUTYL 4-(5-FORMYLPYRID-2-YL)PIPERAZINE-1-CARBOXYLATE-->2,4-DIPHENYL-1,3-THIAZOLE-5-CARBALDEHYDE-->N-BOC-L-Prolinal-->2-[4-(TRIFLUOROMETHYL)PHENYL]-1,3-THIAZOLE-4-CARBALDEHYDE-->4-METHYL-2-[4-(TRIFLUOROMETHYL)PHENYL]-1,3-THIAZOLE-5-CARBALDEHYDE

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